This method is included in NEMI for informational purposes as it is approved by EPA for regulatory use. Detailed information on this method is not currently. eropoly acid. This is reduced to silicomolybdenum blue that is determined pho- tometrically. The method is analogous to APHA SiO2 D+E, ASTM D, . Find the most up-to-date version of ASTM D at Engineering
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Quality Control QC Under certain conditions, silica forms troublesome silica and silicate scales, particularly on high-pressure steam turbine blades. A direct reading spectrophotometer or? It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
For measurements made at wstm, silica concentration may be read directly in milligrams SiO2 per litre from the calibration curve prepared in ASTM D95 – When working with low concentrations of silica, a batch of ammonium molybdate known to produce reasonable blanks, linearity, and reproducibility should be set aside for this purpose.
Refer to Appendix X1 for historical information.
For seawater or brines, this test method is applicable only if matched matrix standards or standard addition techniques are employed. Active view current version of standard Translated Standard: High blanks, nonlinear calibration curves, and poor reproducibility have been observed with d8559 batches of this compound. Due to the complexity of silica chemistry, the form of silica measured is defined by the analytical method as molybdate-reactive silica.
Link to Active This link will always route to the current Active version of the standard. This standard is subject to revision at any time by the responsible technical committee and must be reviewed every?
Standard Test Method for Silica in Water
Note 1—For many natural waters, a measurement of molybdate-reactive silica by this test method provides a close approximation of total silica, and, in practice, the colorimetric method is frequently substituted for other more time-consuming techniques. Asgm is particularly applicable to treated industrial waters.
For standards in the 0. For zstm natural waters, a measurement of molybdate-reactive silica by this test method provides a close approximation of total silica, and, in practice, the colorimetric method is frequently substituted for other more time-consuming techniques.
ASTM D 水中硅测定的标准方法_百度文库
Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard. In cooling water systems, silica forms deposits when solubility limits are exceeded. The upper limit for acceptable precision and the range of acceptable recoveries are detailed below: Prepare a blank using a Such waste waters may ast, contain organic compounds that may interfere in the color formation.
The residue is weighed before and after volatilization as silicon tetra? If non-detects are d85 in all the samples to be analyzed, a Matrix Spike Duplicate should be run instead. It is the responsibility of the user of this standard to establish aastm safety and health practices and determine the applicability of regulatory limitations prior to use.
It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
ASTM D859 – 16
Individual reprints single or multiple copies of this standard may be obtained by contacting ASTM at the above address or at phonefaxor service astm. For seawater or brines, this test method is applicable only if matched matrix standards or standard addition techniques are employed. Refer to Appendix X1 for historical information.
Originally approved in Silica removal is commonly accomplished by ion exchange, distillation, reverse osmosis, or by precipitation, usually with magnesium adtm in a hot or cold lime softening process. It is found as the oxide in crystalline forms, as in quartz; combined with other oxides and metals in a variety of silicates; and in amorphous 1 This test method is under the jurisdiction of ASTM Committee D19 on Water and is the direct responsibility of Subcommittee D The lower limit of this asm is 5 mg of silica.
Active view current version ast, standard. No other units of measurement are included in this standard. For seawater or brines, this test method is applicable only if matched matrix standards or standard addition techniques are employed. Shelf life of this reagent may be extended by refrigeration. The mean and standard deviation of the seven values should then be calculated and compared, according to Practice D aetm, to the single operator precision and recovery established for this Test Method.
ASTM D – 16 – Standard Test Method for Silica in Water
Spike a portion of a water or other sample from each batch with the method analytes at the level of the IDP solution. The presence of most silica in natural waters comes from the gradual degradation of silica-containing minerals. Those forms of silica that are molybdate-reactive include dissolved simple silicates, monomeric silica and silicic acid, and an undetermined fraction of polymeric silica.
After dissolving, add aastm solution to mL of a solution containing 30 g of sodium hydrogen sul? Discard when the color darkens or a precipitate forms.
Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard.
Silicon is the most abundant element in igneous rocks and is the characteristic element of all important rocks except the carbonates. Link to Active This link will always route to the current Active version of the standard.
Precision and Bias 5 No other units of measurement are d8599 in this standard. This adtm method is useful for concentrations as low as 20? Make up to mL with water and store in a dark, plastic bottle. For measurements at nm, plot absorbance versus milligrams SiO2 per litre.
It is found as the oxide in crystalline forms, as in quartz; combined with other oxides and metals in a variety of silicates; and in amorphous forms.